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245 0 0 _aMicroreactors in preparative chemistry :
_bpractical aspects in bioprocessing, nanotechnology, catalysis and more /
_cedited by Wladimir Reschetilowski.
250 _aFirst edition.
264 1 _aWeinheim, Germany :
_bWiley-VCH,
_c[2013]
264 4 _c©2013
300 _a1 online resource (xv, 335 pages) :
_billustrations
336 _atext
_btxt
_2rdacontent
337 _acomputer
_bc
_2rdamedia
338 _aonline resource
_bcr
_2rdacarrier
500 _aEdition statement from running title area.
504 _aIncludes bibliographical references and index.
505 0 _aMicroreactors in Preparative Chemistry: Practical Aspects in Bioprocessing, Nanotechnology, Catalysis and more; Contents; Preface; List of Contributors; 1 Principles of Microprocess Technology; 1.1 Introduction; 1.2 History; 1.3 Basic Characteristics; 1.3.1 Microfluidics and Micromixing; 1.3.2 Temperature and Pressure Control; 1.3.3 Safety and Ecological Impact; 1.4 Industrial Applications; 1.5 Concluding Remarks; References; 2 Effects of Microfluidics on Preparative Chemistry Processes; 2.1 Introduction; 2.2 Mixing; 2.3 Heat Management; 2.3.1 Heat Transfer in Continuous-Flow Devices.
505 8 _a2.3.2 Heat Control of Microchannel Reactors2.4 Mass Transfer and Chemical Reactions; 2.4.1 Fluid-Solid Catalytic Systems; 2.4.2 Fluid-Fluid Systems; 2.4.2.1 Flow Regimes; 2.4.2.2 Mass Transfer; 2.4.3 Three-Phase Systems; 2.4.3.1 Gas-Liquid-Solid Systems; 2.4.3.2 Gas-Liquid-Liquid Systems; 2.5 Flow Separation; 2.5.1 Geometrical Modifications; 2.5.2 Wettability-Based Flow Splitters; 2.5.3 Conventional Separator Adapted for Microstructured Reactors; 2.6 Numbering-Up Strategy; 2.7 Practical Exercise: Experimental Characterization of Mixing in Microstructured Reactors; References.
505 8 _a3 Modular Micro- and Millireactor Systems for Preparative Chemical Synthesis and Bioprocesses3.1 Introduction; 3.2 Modular Microreaction System; 3.3 Examples for Microreactor Applications; 3.3.1 Synthesis of Vitamin A Acetate; 3.3.2 Screening of Process Parameters for a Suzuki-Miyaura Reaction; 3.3.3 Scale-Up of Thermal Rearrangement of Furfuryl Alcohol; 3.3.4 Online Reaction Monitoring and Automation of Chemical Synthesis and Bioprocesses; 3.4 Laboratory Exercise: Suzuki Reaction in a Modular Microreactor Setup; References.
505 8 _a4 Potential of Lab-on-a-Chip: Synthesis, Separation, and Analysis of Biomolecules4.1 Introduction; 4.2 Learning from Nature: Analogies to Living Cells; 4.3 Microenzyme Reactors; 4.3.1 Enzyme Immobilization on the Microchannel Surface; 4.3.2 Enzyme Immobilization on Supports; 4.3.3 Modes of Operation; 4.3.4 Enzymatic Conversions; 4.3.5 Enzymatic Cleavage of Peptides; 4.3.6 Determination of Inhibitor Properties; 4.3.7 Cytotoxicity Assessment; 4.4 Microchip Electrophoresis; 4.4.1 Peptide Analysis; 4.4.2 Chiral Separation; 4.4.3 Coupling Biocatalysis and Analysis.
505 8 _a4.4.4 Determination of Amino Acids in Goods and Foods4.5 Microenzyme Membrane Reactor/Micromembrane Chromatography; 4.6 Nucleic Acid Analysis in Microchannels; 4.7 Saccharide Analyses in Microdevices; 4.8 Practical Exercise: Lipase-Catalyzed Esterification Reaction; References; 5 Bioprocessing in Microreactors; 5.1 Introduction; 5.2 Background; 5.2.1 Basic Elements of a Biosensor; 5.2.2 Different Sensing Methods; 5.2.3 The Effect of Reducing Dimensionality and Length Scales of Biosensors; 5.2.4 Biosensors Based on Field-Effect Transistors; 5.2.4.1 The Main Working Principle of FET Sensors.
520 _aThis is the first book in the field to focus on these aspects, providing extremely valuable information unavailable elsewhere for anyone seeking the practical application of microreactor technology in preparative chemistry. The topics covered branch out in three different directions. To begin with, the knowledge necessary for the preparative chemistry concerning the influence of the so-called microeffects on the reaction procedure and on mass and heat transfer as well as the surface phenomena are provided in detail. Next, practical aspects of the synthesis of various basic chemicals and fi.
588 0 _aPrint version record.
650 0 _aMicroreactors.
650 0 _aChemistry.
_959425
650 7 _aSCIENCE
_xChemistry
_xIndustrial & Technical.
_2bisacsh
650 7 _aTECHNOLOGY & ENGINEERING
_xChemical & Biochemical.
_2bisacsh
650 7 _aChemistry.
_2fast
_0(OCoLC)fst00853344
_959425
650 7 _aMicroreactors.
_2fast
_0(OCoLC)fst01020042
655 4 _aElectronic books.
700 1 _aReschetilowski, Wladimir.
773 0 _tWiley e-books
776 0 8 _iPrint version:
_tMicroreactors in preparative chemistry.
_dWeinheim : Wiley-VCH, 2013
_z9783527332823
_w(OCoLC)847542514
856 4 1 _uhttps://eresourcesptsl.ukm.remotexs.co/user/login?url=https://doi.org/10.1002/9783527652891
_zWiley Online Library
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_b2022-11-04
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